Abstract
A technology for duplex plasma treatment of the steel surface is proposed. At the first stage, it is proposed to carry out nitrocarburising at the cathode polarity of the treated sample to harden the surface layer. The composition and structure of nitrocarburised layers have been studied. It is shown that as a result of the simultaneous diffusion of nitrogen and carbon, their diffusion coefficients increase, contributing to the achievement of concentrations up to 0.74 ± 0.14% and 0.67 ± 0.18%, respectively, as well as an increase in the microhardness of the surface layer to 1020 ± 20 HV. At the second stage, it is proposed to carry out anodic polishing of the nitrocarburised surface to remove the porous oxide layer with a highly developed relief, which is formed as a result of exposure to the surface of electrical discharges and high-temperature oxidation. Tribological tests have shown a joint positive effect of the hardness of the diffusion layer and low surface roughness, including a dense layer of iron oxides, on a reduction in the friction coefficient by a factor of 2 and weight wear by a factor of 23 during fatigue wear of the treated sample under boundary friction and plastic contact with the counterbody.
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References
Yerokhin A L, Nie X, Leyland A, Matthews A, and Dowey S, Surf Coat Technol 122 (1999) 73. https://doi.org/10.1016/S0257-8972(99)00441-7.
Aliofkhazraei M, Macdonald D D, Matykina E, Parfenov E V, Egorkin V S, Curran J A, Troughton S C, Sinebryukhov S L, Gnedenkov S V, Lampke T, Simchen F, and Nabavi H F, Appl Surf Sci Adv 5 (2021) 100121. https://doi.org/10.1016/j.apsadv.2021.100121.
** S, Ma X, Wu R, Wang G, Zhang J, Krit B, Betsofen S, and Liu B, Appl Surf Sci Adv 8 (2022) 100219. https://doi.org/10.1016/j.apsadv.2022.100219.
Bogdashkina N L, Gerasimov M V, Zalavutdinov R K, Kasatkina I V, Krit B L, Lyudin V B, Fedichkin I D, Shcherbakov A I, and Apelfeld A V, Surf Eng Appl Electrochem 54 (2018) 331. https://doi.org/10.3103/S106837551804004X.
P.N. Belkin, S.A. Kusmanov, and E.V. Parfenov, Appl Surf Sci Adv 1 (2020) 100016. DOI: https://doi.org/10.1016/j.apsadv.2020.100016.
Belkin P N, Yerokhin A L, and Kusmanov S A, Surf Coat Technol 307 (2016) 1194. https://doi.org/10.1016/j.surfcoat.2016.06.027.
Belkin V S, Belkin P N, Krit B L, Morozova N V, and Silkin S A, J Mat Eng Perform 29 (2020) 564. https://doi.org/10.1007/s11665-019-04521-1.
Kusmanov S A, Kusmanova Y V, Smirnov A A, and Belkin P N, Mat Chem Phys 175 (2016) 164171. https://doi.org/10.1016/j.matchemphys.2016.03.011.
Rastkar A R, and Shokri B, Surf Interface Anal 44 (2012) 342. https://doi.org/10.1002/sia.3808.
Tsotsos C, Yerokhin A L, Wilson A D, and Leyland A, Wear 253 (2002) 986. https://doi.org/10.1016/S0043-1648(02)00225-9.
Kazerooniy N A, Bahrololoom M E, Shariat M H, Mahzoon F, and Jozaghi T, J Mater Sci Technol 27 (2011) 906. https://doi.org/10.1016/S1005-0302(11)60163-1.
Skakov M, Rakhadilov B, Scheffner M, Karipbaeva G, and Rakhadilov M, Appl Mech Mater 379 (2013) 161. https://doi.org/10.4028/www.scientific.net/AMM.379.161.
Skakov M, Verigina L, and Scheffner M, Appl Mech Mater 698 (2015) 439. https://doi.org/10.4028/www.scientific.net/AMM.698.439.
Zarchi M K, Shariat M H, Dehghan S A, and Solhjoo S, J Mater Res Technol 2 (2013) 213. https://doi.org/10.1016/j.jmrt.2013.02.011.
Jiang Y F, Geng T, Bao Y F, and Zhu Y, Surf Coat Technol 216 (2013) 232. https://doi.org/10.1016/J.SURFCOAT.2012.11.050.
Kusmanov S A, Silkin S A, Smirnov A A, and Belkin P N, Wear 386 (2017) 239. https://doi.org/10.1016/j.wear.2016.12.053.
Kusmanov S A, Tambovskiy I V, Korableva S S, Dyakov I G, Burov S V, and Belkin P N, J Mat Eng Perform 28 (2019) 5425. https://doi.org/10.1007/s11665-019-04342-2.
Smirnov A A, Kusmanov S A, Kusmanova I A, and Belkin P N, Surf Eng Appl Electrochem 53 (2017) 413–418. https://doi.org/10.3103/S106837551705012X.
Mukhacheva T L, Kalinina T M, and Kusmanov S A, J Phys Conf Ser 2144 (2021) 012031. https://doi.org/10.1088/1742-6596/2144/1/012031.
Mukhacheva T L, Belkin P N, Dyakov I G, and Kusmanov S A, Wear 462 (2020) 203516. https://doi.org/10.1016/j.wear.2020.203516.
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This work was financially supported by the Russian Science Foundation (Contract No. 18–79-10094) to the Kostroma State University.
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Kusmanov, S.A., Tambovskiy, I.V., Mukhacheva, T.L. et al. Improved Wear Resistance of Low Carbon Steel by Duplex Surface Treatment Combining Cathodic Plasma Electrolytic Nitrocarburising and Anodic Plasma Electrolytic Polishing. Trans Indian Inst Met 76, 2183–2192 (2023). https://doi.org/10.1007/s12666-023-02921-5
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DOI: https://doi.org/10.1007/s12666-023-02921-5