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Comparison of In Situ Micromechanical Strain-Rate Sensitivity Measurement Techniques

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Abstract

Strain-rate sensitivity (SRS) measurements using transient small-scale techniques are becoming increasingly popular for investigating nanostructured films and microcomponents since they can provide fundamental insights into the plastic deformation mechanisms within small volumes of material. Previously, researchers have typically used either nanoindentation or microcompression strain-rate jump tests on a variety of nanostructured materials and compared the resultant values with bulk compression data as a reference. However, no systematic comparison of the different transient micromechanical techniques has been performed on the same material to establish their relative merits or the consistency of their results. In this study, the SRS of nanocrystalline nickel is investigated using three independent, in situ, transient experimental techniques: miniature tension, nanoindentation, and micropillar compression. The obtained SRS exponents m measured by all techniques were found to be in good agreement, and the resulting apparent activation volume V app of approximately 10 b 3 is consistent with grain boundary diffusion processes and dislocation glide-based plasticity.

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Acknowledgements

The authors want to thank G. Bürki and A. Böll for technical assistance with the miniature tensile stage and the SEM indenter, and they thank N. Siegfried for performing the GDOES measurements. Funding by the Commission for Technology and Innovation (CTI) within the Project No. 209673 is gratefully acknowledged. G. Mohanty and G. Guillonneau would like to acknowledge funding from the EMPA post-doctoral fellowship program NANOCREEP cofunded by FP7: Marie Curie Actions.

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Authors and Affiliations

  1. Laboratory for Mechanics of Materials and Nanostructures, Empa, Swiss Federal Laboratories for Materials Science and Technology, 3602, Thun, Switzerland

    Juri Wehrs, Gaurav Mohanty, Gaylord Guillonneau, Aidan A. Taylor, Xavier Maeder, Damian Frey, Laetitia Philippe, Jeffrey M. Wheeler & Johann Michler

  2. Tribology and Interface Chemistry Group, Materials Institute, École Polytechnique Fédérale de Lausanne, 1015, Lausanne, Switzerland

    Stefano Mischler

  3. Laboratory for Nanometallurgy, Department of Materials Science, ETH Zürich, 8093, Zurich, Switzerland

    Jeffrey M. Wheeler

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  1. Juri Wehrs
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Correspondence to Juri Wehrs.

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Wehrs, J., Mohanty, G., Guillonneau, G. et al. Comparison of In Situ Micromechanical Strain-Rate Sensitivity Measurement Techniques. JOM 67, 1684–1693 (2015). https://doi.org/10.1007/s11837-015-1447-z

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  • DOI: https://doi.org/10.1007/s11837-015-1447-z

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