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Article
Novel Method for Spectrophotometric Determination of L-Tryptophan in the Enzymatic Resolution of DL-N-Acetyl-Tryptophan
A novel spectrophotometric method for the determination of tryptophan (Trp) has been proposed. The sensitive and simple method was based upon the finding that NaNO2 and Trp formed a diazotized product in nitric a...
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Article
A papaya-specific gene, papain, used as an endogenous reference gene in qualitative and real-time quantitative PCR detection of transgenic papayas
Genetically modified (GM) papaya lines have been approved for commercialization and are widely cultivated in many countries. As a step towards the development of reliable qualitative and quantitative PCR metho...
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Article
Cloud-Point Extraction Combined with LC–MS for Analysis of Memantine in Rat Plasma
The feasibility of using cloud-point extraction as a simple and effective means of recovery of memantine from rat plasma before LC–MS analysis has been demonstrated. A non-ionic surfactant Triton X-114 was use...
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Article
Comparison of Different Silica-Based Imidazolium Stationary Phases for LC in Separation of Alkaloids
Three stationary phases based on silica modified with imidazolium ionic liquids were prepared and characterized for their use in high-performance liquid chromatography. Multiple interactions of separation mech...
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Article
Enantioselective Separation and Determination of Carnosine in Rat Plasma by Fluorescence LC for Stereoselective Pharmacokinetic Studies
A sensitive fluorescence liquid chromatographic analytical method was developed for the simultaneous determination of carnosine enantiomers in rat plasma. The method was applied to pharmacokinetic studies. Chi...
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Article
Molecular imprinting in ionic liquid-modified porous polymer for recognitive separation of three tanshinones from Salvia miltiorrhiza Bunge
Five ionic liquid-modified porous polymers with different imidazolium-based functional groups were obtained. A molecular imprinting technique was introduced to form the ordered functional groups in the porous ...
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Article
Three-Phase Solvent Bar Microextraction Combined with HPLC for Extraction and Determination of Plasma Protein Binding of Bisoprolol
A three-phase solvent bar microextraction (TPSBME) technique combined with high performance liquid chromatography (HPLC)–fluorescence detection was evaluated for the quantitative determination of plasma protei...
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Article
Quantitative profiling of tryptophan metabolites in serum, urine, and cell culture supernatants by liquid chromatography–tandem mass spectrometry
A sensitive, selective, and comprehensive method for the quantitative determination of tryptophan and 18 of its key metabolites in serum, urine, and cell culture supernatants was developed. The analytes were s...
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Article
Simultaneous Determination of 15 Plant Growth Regulators in Bean Sprout and Tomato with Liquid Chromatography–Triple Quadrupole Tandem Mass Spectrometry
The present paper describes the development and validation of a new reversed-phase liquid chromatography–electrospray ionization tandem mass spectrometric method for determination of 15 plant growth regulators...
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Article
A SERS-based immunoassay for porcine circovirus type 2 using multi-branched gold nanoparticles
We report on a facile immunoassay for porcine circovirus type 2 (PCV2) based on surface enhanced Raman scattering (SERS) using multi-branched gold nanoparticles (mb-AuNPs) as substrates. The mb-AuNPs in the im...
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Article
Deep Eutectic Solvent-Based HS-SME Coupled with GC for the Analysis of Bioactive Terpenoids in Chamaecyparis obtusa Leaves
Headspace-solvent microextraction (HS-SME) was developed as a solvent-minimized extraction technique, but few studies have examined the applications of deep eutectic solvents (DESs) to the HS-SME of bioactive ...
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Article
Efficient carbon dioxide electrolysis based on ceria cathode loaded with metal catalysts
Fluorite-type heterogeneous catalyst ceria is a mixed conductor and widely used as a hydrocarbon-fueled solid oxide fuel cell anode because of its advantage of anti-carbon deposition, redox stability, and ther...
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Article
Colorimetric and visual determination of total nereistoxin-related insecticides by exploiting a nereistoxin-driven aggregation of gold nanoparticles
We describe a method for the visual and colorimetric determination of total nereistoxin-related insecticide residues. It is based on the nereistoxin-induced aggregation of gold nanoparticles (AuNPs). The nerei...
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Article
Fluorescence aggregation assay for the protein biomarker mucin 1 using carbon dot-labeled antibodies and aptamers
We have developed a sensitive fluorescence assay for the protein biomarker mucin 1 (MUC1). It is based on the aggregation of functionalized carbon dots (CDs) in the presence of MUC1. The CDs with a size of ~2 ...
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Article
Synthesis of a graphitic carbon nitride nanocomposite with magnetite as a sorbent for solid phase extraction of phenolic acids
We have developed a facile in-situ growth method for the deposition of magnetite (Fe3O4) particles on the surface of a graphitic carbon nitride (g-C3N4) nanosheet. The material was characterized by X-ray diffract...
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Article
Simultaneous Separation and Determination of 22 Coumarin Derivatives in Cosmetics by UPLC-MS/MS
A comprehensive analytical method based on ultra-performance liquid chromatography coupled with tandem mass spectrometry (UPLC-MS/MS) has been developed for the simultaneous determination of 22 regulated couma...
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Article
Development of a Detection Kit Based on G-Quadruplex DNAzyme for Detection of Lead(II) Ion in Food Samples
The biocatalytic function of G-quadruplex DNAzyme has been first used to design a detection kit for colorimetric detection of Pb2+ in food samples by coupling guaiacol (GA) as an effective and ideal colorimetric ...
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Article
Numerical simulation of deflagration to detonation transition in granular HMX explosives under thermal ignition
To study the deflagration to detonation transition process in granular explosive under thermal ignition condition, the conductive burning is introduced into the classical model. The novel space–time conservati...
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Article
Nucleation ability of nonmetallic organophosphate derivatives in isotactic polypropylene
Nonmetallic organophosphate derivatives of ammonium (An), triethylammonium (CAn), and quaternary phosphonium (SP) salts of 2,2′-methylene-bis-(4,6-di-tert-butylphenyl) phosphate were synthesized and characterized...
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Article
Dual signal amplification strategy for amperometric aptasensing using hydroxyapatite nanoparticles. Application to the sensitive detection of the cancer biomarker platelet-derived growth factor BB
The authors describe a dual signal amplification strategy for improving the sensitivity of electrochemical aptasensor. Hydroxyapatite nanoparticles (HAP-NPs) serve as the support for deposition of the respecti...