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ULM-12 and ULM-19: The Hydrated and Anhydrous forms of the First Synthetic Oxyfluorinated Iron Phosphate with an Open Structure
ULM-19 or [Fe4(PO4)4F2], [C6H14N2] was obtained in a monocrystalline form from the dehydration of single crystals of ULM-12, or [Fe4(PO4)4F2(H2O)3], [C6H14N2] at 260°C. It is monoclinic (S.G. P21/n) with a = 10.0...