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Article
Solid-phase peptide synthesis: from standard procedures to the synthesis of difficult sequences
This protocol for solid-phase peptide synthesis (SPPS) is based on the widely used Fmoc/tBu strategy, activation of the carboxyl groups by aminium-derived coupling reagents and use of PEG-modified polystyrene ...
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Chapter and Conference Paper
N,O-Acyl Shifts: Unexpected Side-Reaction and Beneficial Tool in Fmoc-Chemistry
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Chapter
Protected amino acid chlorides: Coupling reagents suitable for the most highly hindered systems
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Chapter
Efficient assembly of stable site-directed fluorescence labeled peptides
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Article
Influence of proline and β-turn mimetics on the cyclization of penta- and hexapeptides
Proline and Pro-derived peptidomimetics, such as meoxPro-Oic (4-methoxy-proline-octahydro indolic acid), and DBF (2-aminoethyl-6-dibenzofuran propionic acid) were introduced into thymopentin-derived penta- [SP...
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Article
Influence of proline and β-turn mimetics on the cyclization of penta- and hexapeptides
Proline and Pro-derived peptidomimetics, such as meoxPro-Oic (4-methoxy-proline-octahydro indolic acid), and DBF (2-aminoethyl-6-dibenzofuran propionic acid) were introduced into thymopentin-derived penta-[SP5...
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Article
Synthesis of Fmoc-amino acid fluorides via DAST, an alternative fluorinating agent
DAST [(diethylamino)sulfur trifluoride] has shown to be an excellent alternative fluorinating agent for synthesis of Fmoc-amino acid fluorides. The use of DAST is advantageous relative to other fluorinating ag...
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Chapter
Tritium Labeling of Brain Peptides
During the past decade, radiolabeling of biologically active peptides has become a widely applied and essential technique for a variety of biochemical and physiological investigations.