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Synthesis, structure and ethylene polymerization behavior of titanium complexes [C3H6(N = CH™Ar™O)2]TiCl2
The reaction of C3H6(N=CH-Ar-OH)2 (Ar = 5-tert-butyl-C6H3 (2a), 3-tert-butyl-C6H3 (2b), 3-methyl-C6H3 (2c)) with 2 equiv. of BuLi followed by 1 equiv TiCl4 yields the dichloride complexes [C3H6(N=CH-Ar-O)2]TiCl2[...