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Article
Synthesis, structures and properties of two novel copper(II) complexes with hydrogen bonding supramolecular networks
Two novel complexes, [Cu(HL)2(H2O)]2(OH)2(ClO4)2·1.5H2O (1) and [Cu(HL)2]Cl2·4H2O (2), have been prepared by reacting copper salts with the 4-amino-3-ethyl-1,2,4-triazole-5-thione (HL) ligand in neutral solution ...
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Article
Highly enantioselective trap** of zwitterionic intermediates by imines
Reactions with the unstable and highly reactive zwitterionic intermediates generated in processes catalysed by transition metals are providing new opportunities for molecular constructions. Insertion reactions...
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Article
Exploring antibiotic resistant mechanism by microcalorimetry II
In an effort to understand the reaction of antibiotic hydrolysis with B2 metallo-β-lactamases (MβLs), the thermodynamic parameters of imipenem hydrolysis catalyzed by metallo-β-lactamase ImiS from Aeromonas veron...
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Article
Exploring antibiotic resistance based on enzyme hydrolysis by microcalorimetry
In an effort to understand the reactions of antibiotics hydrolysis with metallo-β-lactamases (MβLs), the thermokinetic parameters of cefazolin hydrolysis with B1 subclass MβL CcrA from Bacteroides fragilis were d...
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Article
Recovery of titania from high titanium slag by roasting method using concentrated sulfuric acid
By means of energy-dispersive X-ray spectroscopy (EDX) and scanning electron microscope (SEM) analysis, the phase structure characteristics of high titanium slag were analyzed. Through the single factor and th...
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Article
Effects of Pulsed Current and Pulsed Magnetic Field Complex Pretreatment on Martensite Transformation of Cr5 Steel during Continuous Cooling
Carbide precipitation and martensite transformation in Cr5 steel have been observed in situ by high-temperature confocal laser-scanning microscopy. In this way, the influences of pulsed current and pulsed magn...
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Article
The influence of perchloric acid on 2,3-dimethylpyrazine and 1,2-bis(4-pyridyl)ethane: crystal structure and Hirshfeld surfaces analysis
2,3-Dimethylpyrazine and 1,2-bis(4-pyridyl)ethane are both N-containing aromatic heterocyclics with two N atoms approximately in the para position. We here report two compounds derived from these heterocyclics...
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Article
An efficient and high-yielding protocol for the production of Regorafenib via a new synthetic strategy
An improved, high-yielding, and efficient protocol for the production of Regorafenib (1), a novel diaryl urea inhibitor of multiple protein kinases, is described. The highlight of the process chemistry design and...
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Article
Co-crystallization of a benzimidazole derivative with carboxylic acids
The co-crystallization of a benzimidazole derivative (1, C27H26N6O3, 3-[[[2-[[(4-Cyanophenyl) amino]methyl]-1-methyl-1H-benzimidazol-5-yl]carbonyl]pyridin-2-ylamino]propionic acid ethyl ester), with fumaric acid ...
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Article
Compatibility study of rivaroxaban and its pharmaceutical excipients
Rivaroxaban is an oral direct Factor Xa inhibitor to treat thrombus. The aim of this study is to investigate the drug–excipient compatibility between rivaroxaban tablet and pharmaceutical excipients by a combi...
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Article
Influence of pulsed magneto-oscillation on microstructure and mechanical property of rectangular 65Mn steel ingot
The pulsed magneto-oscillation (PMO) technique has the potential to be applied in the production of heavy steel ingot. In order to confirm it and achieve more insights, the solidification of rectangular 65Mn s...
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Article
Interactions of phosphorylated cyclohexapeptides with uranyl: insights from experiments and theoretical calculations
Two phosphorylated cyclohexapeptides (CPs) bearing one (CP1) or two phosphates (CP2) were synthesized to explore the interactions between uranyl ions and very small cyclic peptides. According to the results of...
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Article
Ore-blending optimization for Canadian iron concentrate during iron ore sintering based on high-temperature characteristics of fines and nuclei
Canadian iron concentrate (CIC) can elevate the ferrous grade and lower the contents of gangue components and harmful elements in the sinter. To understand high-temperature characteristics of CIC and typical i...
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Article
Hierarchical porous hard carbon enables integral solid electrolyte interphase as robust anode for sodium-ion batteries
Hard carbon is the most promising anode for sodium-ion battery applications due to the wide availability and low work voltage. However, it often delivers worse electrochemical performance in ester-based electr...
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Article
Inhibition of coal spontaneous combustion by an environment-friendly, water-based fire extinguishing agent
At present, inhibitors have been widely used in the field of coal fire prevention and control, but there are some defects in the use of them. So it is necessary to find a new practical and economical inhibitor...
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Article
Plasmonic photo-assisted electrochemical sensor for detection of trace lead ions based on Au anchored on two-dimensional g-C3N4/graphene nanosheets
In this paper, a plasmonic photo-assisted electrochemical sensor, Au anchored on two-dimensional (2D) graphitic carbon nitride (g-C3N4)/reduced graphene oxide (rGO) nanosheets (Au/g-C3N4/rGO), was facile fabricat...
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Article
Investigation of reheat cracking susceptibility in CGHAZ of modified T23 steel
T23 steel (2.25Cr–1Mo–1.6W–0.24V–0.05Nb, in wt.%) has been widely used as water walls in ultra-supercritical (USC) power plants. However, high reheat cracking susceptibility of T23 steel hazarded the safety of...
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Article
Effects of pulse magneto-oscillation on GCr15 bearing steel continuous casting billet
Pulse magneto-oscillation (PMO) added during solidification could affect the solidification structure and macrosegregation. A modified thermal simulation equipment was applied to prepare GCr15 bearing steel co...
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Article
A facile and non-destructive quartz fiber shadow mask process for the sub-micrometer device fabrication on two-dimensional semiconductors
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Article
Preparation of magnetic hematite/carbon nanoscrolls composite photocatalysts and its performance in photocatalytic N2/H2O synthesis of ammonia
In this paper, coal-based carbon nanoscrolls (CNS) were prepared using coal from Wucaiwan Coal Mine in **njiang as a carbon source: first, most of the impurities in the coal were removed by acid treatment; the...