![Loading...](https://link.springer.com/static/c4a417b97a76cc2980e3c25e2271af3129e08bbe/images/pdf-preview/spacer.gif)
-
Article
Synthesis, Structure and DNA-Binding Studies of Oxamido-Bridged Binuclear Copper(II) Complex: [Cu2(heap)](bipy)(ClO4)2
A new μ-oxamido-bridged copper(II)–copper(II) binuclear complex with formula of [Cu2(heap)](bipy)(ClO4)2, where H2heap and bipy are N,N′-bis(N-hydroxyethylaminopropyl)-oxamide and 4,4′-bipyridine, respectively, h...
-
Article
Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide
(S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide was synthesized from Cbz-l-proline through two steps and characterized by NMR and MS. The crystal structure was determined from single-crystal X-ray diffraction da...
-
Article
Synthesis and Crystal Structure of [Ni(L)(Phen)(H2O)]·3.75H2O
The title compound, [Ni(L)(Phen)(H2O)]·3.75H2O, where L = (E)-2-(5-formyl-2-oxidobenzylideneamino)ethanesulfonate, was synthesized in aqueous methanol in the presence of Ni(II), Phen and the potassium salt of 2-{...
-
Article
Syntheses and Crystal Structures of Two Novel 1D Complexes of Zinc(II) with Terephthalato-bridge
Two novel complexes [Zn(NIT3-py)(tp)]n 1 and [Zn(im3-py)(tp)]n 2 (NIT3-py = 2-(3′-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide, im3-py = 2-(3′-pyrid...
-
Article
The hydrogen bonding in 2-amino-3-cyano-4-(3-nitrophenyl)-4,6-dihydro-5H-pyrano[3,2-c]quinolin-5-one N,N-dimethylformamide solvate monohydrate
The crystal structure of 2-amino-3-cyano-4,6-dihydro-4-(3-nitrophenyl)-5H-pyrano[3,2-c]quinolin-5-one N,N-dimethylformamide solvate monohydrate is determined by room temperature X-ray diffraction. The title compo...
-
Article
Unclassical hydrogen bonds of C—H⋅sO and C—H⋅sN in the crystals of 2-amino-3-cyano-4-(3,4-dichlorophenyl)-5-oxo-1,4,5,6-tetrahydro-4H-pyrano[2,3-d]pyrimidine
The 2-amino-3-cyano-4-(3,4-dichlorophenyl)-5-oxo-1,4,5,6-tetrahydro-4H-pyrano[2,3-d] pyrimidine (1, C17H15Cl2N5O3) was synthesized and characterized by IR,1H NMR and elemental analysis. The molecular structure of
-
Article
Crystal structures and spectroscopic properties of copper(II) and zinc(II) complexes with the macrocycle 1,4,7-tris(2-pyridylmethyl)-1,4,7-triazacyclononane
Two novel transition-metal copper and zinc complexes [(CuL)2]·(ClO4) (1) and [(ZnL)]·(ClO4)2 (2) (L = 1,4,7-tris(2-pyridylmethyl)-1,4,7-triazacyclononane) have been synthesized and structurally determined. The tw...
-
Article
Crystal and molecular structure of a nickel(II) complex with a macrocyclic [14]N4 ligand
The crystal and molecular structure of a macrocyclic oxamido Schiff base Ni(II) complex [NiL] has been determined by X-ray crystallography. L is the dianion of diethyl 5,6,7,8,15,16-hexahydro-6,7-dioxodibenzo[...
-
Article
Synthesis and structure of tris[2-(1-naphthalenyloxy)ethyl]amine and tris[2-(1-naphthalenyloxy)ethyl]amine perchlorate
Syntheses and crystal structures of tris[2-(1-naphthalenyloxy)ethyl]amine 1 and tris[2-(1-naphthalenyloxyl)ethyl]amine perchlorate 2 are reported. Compound 1 crystallizes in the rhombohedral system, space group R
-
Article
Crystal structure of the addition compound of N,N′-bi(2-pyridylmethyl)-oxamide and complex of manganese with 1,10-phenanthroline
The structure of the addition compound, Mn(phen)3(PMoxdH2)(ClO4)2 was established by X-ray crystallography, where PMoxdH2 is N,N′-bi(2-pyridylmethyl)-oxamide. Six nitrogen atoms of the three 1,10-phenanthroline b...
-
Article
A dinuclear cyano-bridged complex based on hexacyanoferrate(III) and samarium(III) nitrate: synthesis and crystal structure
A new complex, [Sm(DMF)4(H2O)4Fe(CN)6]·H2O (DMF = N, N-dimethylformamide), has been synthesized and characterized by X-ray single crystal structure and thermogravimetric analyses. The complex crystallizes in the