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Atomic Absorption Control of Ultimate Allowable Concentration of Elements in Meat Products without Sample Dissolution

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Moscow University Chemistry Bulletin Aims and scope

Abstract

In order to control the maximum levels of As, Cr, Pb, Cd, and Sn in meat products, it is proposed to transfer them to a suspension of 140 mg/mL and use an atomic absorption spectrometer with a graphite furnace, equipped with a probe attachment for a two-stage atomization of the suspension. The working linear range covers 0.2–9 ultimate allowable concentrations. The error is smaller by factors of 2 to 3 than that of the methods with sample dissolution, and it saves at least 12 h in time.

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Notes

  1. w/v is the percentage by weight and volume.

  2. v/v is the percentage by volume.

REFERENCES

  1. TR TS (Technical Regulations of the Customs Union) 021/2011: On the Safety of Food Products, Moscow, 2011, no. 880.

  2. Commission Regulation (EC) no. 1881/2006: Setting Maximum Levels for Certain Contaminants in Foodstuffs, Brussels: European Commission, 2006.

  3. GOST (State Standard) 31671-2012: Foodstuffs. Determination of Trace Elements. Preparation of Samples by Pressure Digestion, Moscow, 2014.

  4. Aras, N.K. and Ataman, O.Y., Trace Element Analysis of Food and Diet, Cambridge: R. Soc. Chem., 2006.

    Google Scholar 

  5. GOST (State Standard) R 51301-99: Foodstuffs and Food Raw Materials. Anodic Strip** Voltammetric Methods of Toxic Traces Elements Determination (Cadmium, Lead, Copper and Zinc), Moscow, 2010.

  6. GOST (State Standard) 31628-2012: Foodstuffs and Food Raw Materials. Anodic Strip** Voltammetric Method of Arsenic Mass Concentration Determination, Moscow, 2014.

  7. GOST (State Standard) 33426-2015: Meat and Meat Products. Determination of Lead and Cadmium by Electrothermal Atomic Absorption Spectrometry, Moscow, 2016.

  8. M (Procedure) 04-64-2017: Food Products and Food Raw Materials. Feed and Raw Materials for Their Production. Method for Measuring the Mass Fraction of Cadmium, Arsenic, Tin, Mercury, Lead, Chromium by Atomic Absorption Spectroscopy Using an Atomic Absorption Spectrometers with Electrothermal Atomization MGA-915, MGA-915M, MGA-915MD, and MGA-1000.

  9. Solid Sample Analysis: Direct and Slurry Sampling Using GF-AAS and ETV-ICP, Kurfürst, U., Ed., Berlin: Springer, 1998.

    Google Scholar 

  10. Schlemmer, G. and Radziuk, B., Analytical Graphite Furnace Atomic Absorption Spectrometry: A Laboratory Guide, Bazel: Birkhäuser Basel, 1999.

  11. GOST (State Standard) R 54639-2011: Foodstuffs and Animal Feeding Stuffs. Determination of Mercury by Zeeman Atomic Absorption Spectrometry, Moscow, 2012.

  12. Viñas, P., Pedro-Martínez, M., and Hernández-Cordoba, M., Anal. Chim. Acta, 2000, vol. 412, p. 121.

    Article  Google Scholar 

  13. Nomura, C.S. and Oliveira, P.V., Quim. Nova, 2006, vol. 29, no. 2, p. 234.

    Article  CAS  Google Scholar 

  14. Gallindo Borges, D.L., Furtado da Silva, A., Welz, B., Curtius, J., and Heitmann, U., J. Anal. At. Spectrom., 2006, vol. 21, p. 763.

    Article  CAS  Google Scholar 

  15. Dami, I.C.F., Silva, M.M., Vale, M.G.R., and Welz, B., Spectrochim. Acta, Part B, 2007, vol. 62, p. 1037.

    Article  Google Scholar 

  16. Welz, B., Becker-Ross, H., Florek, S., and Heitmann, U., High-Resolution Continuum Source AAS: The Better Way to Do Atomic Absorption Spectrometry, Darmstadt: Wiley, 2005.

    Book  Google Scholar 

  17. Zakharov, Yu.A. and Kokorina, O.B., J. Anal. Chem., 2012, vol. 67, no. 8, p. 706. https://doi.org/10.1134/S1061934812080084

    Article  CAS  Google Scholar 

  18. Zakharov, Yu.A., Kokorina, O.B., Khasanova, S.I., Irisov, D.S., and Khaibullin, R.R., Analitika Kontrol’, 2013, vol. 17, no. 3, p. 275.

    Google Scholar 

  19. Zakharov, Yu.A., Okunev, R.V., Khaibullin, R.R., Irisov, D.S., and Sadykov, M.F., Zavod. Lab.,Diagn. Mater., 2014, vol. 80, no. 2, p. 12.

    CAS  Google Scholar 

  20. Petrov, Yu.F., Gudkov, A.Yu., Bagmanova, N.N., Kuznetsov, V.M., Golovny, I.A., El’kind, O.B., and Sudakov, E.V., Ross. Parazitol. Zh., 2009, vol. 4, p. 86.

    Google Scholar 

  21. Narozhnykh, K.N., Strizhkova, M.V., and Konovalova, T.V., Fundam. Issled. Biol. Nauki, 2015, no. 2, p. 2158.

  22. Frolova, O.A., Karpova, M.V., Makhmutova, I.P., and Musin, R.A., Gig. Sanit., 2014, vol. 93, no. 6, p. 72.

    CAS  PubMed  Google Scholar 

  23. Duta, S., Robouch, P., Barbu, L., and Taylor, P., Spectrochim. Acta, Part A, 2007, no. 62, p. 337. https://doi.org/10.1016/j.sab.2007.02.004

  24. Zakharov, Yu.A., Gil’mutdinov, A.K., and Kokorina, O.B., J. Appl. Spectrosc., 2005, vol. 72, no. 1, p. 132. https://doi.org/10.1007/s10812-005-0043-3

    Article  CAS  Google Scholar 

  25. Khaibullin, R.R., Irisov, D.S., Salikhova, O.B., and Zakharov, Yu.A., Opt. Spectrosc., 2019, vol. 126, no. 2, p. 161. https://doi.org/10.1134/S0030400X19020140

    Article  CAS  Google Scholar 

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ACKNOWLEDGMENTS

The authors thank A. Kh. Gilmutdinov and K.Yu. Nagulin for providing the standard samples of biological tissues.

Funding

This work was supported by Kazan (Volga) Federal University and LLC Atzond.

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Correspondence to Yu. A. Zakharov.

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CONFLICT OF INTEREST

The authors declare that they have no conflict of interest.

LIST OF ABBREVIATIONS

MPC, maximum permissible concentration; Sr, standard deviation; P, confidence probability

Additional information

Translated by Sh. Galyaltdinov

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Khaibullin, R.R., Irisov, D.S., Zakirov, A.I. et al. Atomic Absorption Control of Ultimate Allowable Concentration of Elements in Meat Products without Sample Dissolution. Moscow Univ. Chem. Bull. 75, 56–63 (2020). https://doi.org/10.3103/S002713142001006X

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  • DOI: https://doi.org/10.3103/S002713142001006X

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