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Specific Features of the Molecular and Crystalline Structure of Two Crystallosolvates of 4-Amino-N-(4-nitrophenyl)benzenelsulfonamide

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Abstract

Two new crystallosolvates based on 4-amino-N-(4-nitrophenyl)benzenelsulfonamide with dimethyl sulfoxide and N,N-dimethylacetamide have been investigated by X-ray diffraction (XRD) analysis. It is shown that the solvent presence barely affects the molecular structure of the 4-amino-N-(4-nitrophenyl) benzenelsulfonamide compound, which was investigated previously (crystal without solvent), but affects its conformational structure. The intermolecular bond of the NH···O type (solvent molecules) is implemented in both new crystal structures

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REFERENCES

  1. G. L. Perlovich, A. M. Ryzhakov, V. V. Tkachev, and L. Kr. Hansen, Cryst. Growth Des. 11, 1067 (2011).

    Article  Google Scholar 

  2. A. Korolkovas, Essentials of Medicinal Chemistry (Wiley, New York, 1988), p. 699.

    Google Scholar 

  3. D. A. Adsmond and D. J. W. Grant, J. Pharm. Sci. 90 (12), 2058 (2001).

    Article  Google Scholar 

  4. C. J. Kelly, J. M. S. Skakle, J. L. Wardell, et al., Acta Crystallogr. B 58, 94 (2002).

    Article  Google Scholar 

  5. G. M. Sheldrik, SHELX-86, Program for the Crystal Structure Determination (University of Cambridge, Cambridge, England, 1986).

    Google Scholar 

  6. G. M. Sheldrik, SHELXTL Vers. 6.14, Structure Determination Software Suite (Brucker AXS, Madison, Wisconsin, USA, 2000).

    Google Scholar 

  7. A. Parkin, A. Collins, C. J. Gilmore, and C. C. Wilson, Acta Crystallogr. B 64, 66 (2008).

    Article  Google Scholar 

Download references

Funding

The publication was financially supported by the Ministry of Education and Science of the Russian Federation (the Agreement number 02.a03.21.0008).

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Authors and Affiliations

  1. Institute of Problems of Chemical Physics, Russian Academy of Sciences, 142432, Chernogolovka, Moscow oblast, Russia

    V. V. Tkachev & A. N. Utenyshev

  2. Institute of Physiologically Active Substances, Russian Academy of Sciences, 142432, Chernogolovka, Moscow oblast, Russia

    V. P. Kazachenko

  3. Peoples’ Friendship University of Russia (RUDN University), 117198, Moscow, Russia

    O. V. Avramenko

  4. Sechenov First Moscow State Medical University, Ministry of Health of the Russian Federation, 119991, Moscow, Russia

    A. N. Utenyshev

Authors
  1. V. V. Tkachev
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  2. A. N. Utenyshev
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  3. V. P. Kazachenko
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  4. O. V. Avramenko
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Corresponding author

Correspondence to A. N. Utenyshev.

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Translated by Yu. Sin’kov

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Tkachev, V.V., Utenyshev, A.N., Kazachenko, V.P. et al. Specific Features of the Molecular and Crystalline Structure of Two Crystallosolvates of 4-Amino-N-(4-nitrophenyl)benzenelsulfonamide. Crystallogr. Rep. 64, 894–897 (2019). https://doi.org/10.1134/S1063774519060233

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  • DOI: https://doi.org/10.1134/S1063774519060233

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