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Preparation of Iron Ytterbium Garnet by Anion-Exchange Resin Precipitation

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Abstract

Rare-earth ferrite garnets (REFGs) have pronounced magnetic and optical properties and are widely used in magnetooptics, laser and microwave technologies. This work offers a method for producing Yb3Fe5O12 powders with a mean grain size of 47 ± 9 nm, by means of the anion-exchange resin coprecipitation of iron(III) and ytterbium followed by annealing of the product at 1100°C. The anion-exchange resin precipitation rate and optimal parameters have been determined, as well as the parameters of precursors heat treatment. The products have been characterized by chemical analysis, X-ray powder diffraction, differential scanning calorimetry, and electron microscopy. The method is promising for the production of other REFGs and nonferrous metal ferrites.

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ACKNOWLEDGMENTS

Equipment of the Krasnoyarsk Regional Shared Facilities Center, the Krasnoyarsk Scientific Center of the Siberian Branch of the Russian Academy of Sciences, was used in the work.

Funding

This work was fulfilled under the Government assignment to the Institute of Chemistry and Chemical Technologies, the Siberian Branch of the Russian Academy of Sciences (project no. 0287-2021-0014).

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Authors and Affiliations

  1. Institute of Chemistry and Chemical Technology, Siberian Branch of the Russian Academy of Sciences, 660036, Krasnoyarsk, Russia

    S. V. Saikova, E. A. Kirshneva, N. P. Fadeeva, M. V. Panteleeva & E. V. Pikurova

  2. Siberian Federal University, 660041, Krasnoyarsk, Russia

    S. V. Saikova, E. A. Kirshneva & A. S. Samoilo

Authors
  1. S. V. Saikova
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  2. E. A. Kirshneva
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  3. N. P. Fadeeva
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  4. M. V. Panteleeva
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  5. E. V. Pikurova
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  6. A. S. Samoilo
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Corresponding author

Correspondence to S. V. Saikova.

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Translated by O. Fedorova

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Saikova, S.V., Kirshneva, E.A., Fadeeva, N.P. et al. Preparation of Iron Ytterbium Garnet by Anion-Exchange Resin Precipitation. Russ. J. Inorg. Chem. 67, 158–165 (2022). https://doi.org/10.1134/S0036023622020140

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  • DOI: https://doi.org/10.1134/S0036023622020140

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