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Synthesis, crystal and molecular structure of 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane

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Abstract

3,7-Ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane has been found to adopt a chair–chair conformation in the crystalline state in contrast to 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonan-9-one, which had been previously found to exist in a chair-boat conformation.

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Authors and Affiliations

  1. Lomonosov Moscow State University, Moscow, 119991, Russia

    I. V. Grishina, D. V. Makeev, V. B. Rybakov, V. L. Lapteva, V. A. Palyulin & N. S. Zefirov

Authors
  1. I. V. Grishina
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  2. D. V. Makeev
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  3. V. B. Rybakov
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  4. V. L. Lapteva
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  5. V. A. Palyulin
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  6. N. S. Zefirov
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Corresponding author

Correspondence to V. A. Palyulin.

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† Deceased.

Original Russian Text © I.V. Grishina, D.V. Makeev, V.B. Rybakov, V.L. Lapteva, V.A. Palyulin, N.S. Zefirov, 2017, published in Doklady Akademii Nauk, 2017, Vol. 477, No. 1, pp. 48–52.

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Grishina, I.V., Makeev, D.V., Rybakov, V.B. et al. Synthesis, crystal and molecular structure of 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane. Dokl Chem 477, 239–243 (2017). https://doi.org/10.1134/S0012500817110015

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  • DOI: https://doi.org/10.1134/S0012500817110015

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