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Synthesis and the structure of tribromo(7-bromobicyclo[4.1.0]hept-7-yl)germane

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Abstract

A general procedure was developed for the synthesis of halocyclopropylgermanes. This procedure was used for the preparation of tribromo(7-bromobicyclo[4.1.0]hept-7-yl)germane. The molecular structure was established by GLC-mass spectrometry, 1H NMR spectroscopy, and X-ray diffraction analysis.

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Authors and Affiliations

  1. M. V. Lomonosov Moscow State Academy of Fine Chemical Technology, 86 prosp. Vernadskogo, 117571, Moscow, Russian Federation

    A. A. Korlyukov, S. P. Knyazev & E. A. Chernyshev

  2. State Research Center of Russian Federation “State Research Institute of Chemistry and Technology of Organoelement Compounds”, 38 sh. Entuziastov, 111123, Moscow, Russian Federation

    N. V. Alekseev, K. V. Pavlov, O. V. Krivolapova & V. V. Shcherbinin

  3. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian Federation

    M. Yu. Antipin & K. A. Lyssenko

Authors
  1. A. A. Korlyukov
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  2. N. V. Alekseev
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  3. S. P. Knyazev
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  4. E. A. Chernyshev
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  5. K. V. Pavlov
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  6. O. V. Krivolapova
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  7. V. V. Shcherbinin
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  8. M. Yu. Antipin
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  9. K. A. Lyssenko
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Korlyukov, A.A., Alekseev, N.V., Knyazev, S.P. et al. Synthesis and the structure of tribromo(7-bromobicyclo[4.1.0]hept-7-yl)germane. Russian Chemical Bulletin 50, 2203–2205 (2001). https://doi.org/10.1023/A:1015026107353

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  • DOI: https://doi.org/10.1023/A:1015026107353

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