Log in

Effect of Heat Treatment on Microstructure and Properties of Selective Laser Melting AlSi10Mg Alloy

  • Original Research Article
  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

AlSi10Mg alloy was prepared by selective laser melting (SLM) using self-made AlSi10Mg powder as raw material. Optical microscope, scanning electron microscope, electron backscattering instrument, and x-ray diffractometer were used to compare and study the differences of microstructure and properties of AlSi10Mg alloy before and after heat treatment. The results show that the AlSi10Mg alloy formed by SLM is mainly composed of α-Al solid solution and network eutectic Si, and with a small amount of Mg2Si precipitates, the mechanical properties are better than those of traditional casting alloys. The molten pool is composed of fine grain zone, coarse grain zone and heat affected zone. The grain size of each zone is different. The center of the molten pool is mainly equiaxed grains randomly distributed, and the boundary of the molten pool is mainly columnar grains preferentially growing along <111> , forming weak brass texture. With the increase of heat treatment temperature, the reticulate eutectic Si gradually dissolves and breaks into particles, and is further coarsened and spheroidized. The strength and hardness of the alloy decrease and the elongation increases. Columnar grains gradually transform into equiaxed grains, the preferred orientation of grains weakens and the texture gradually disappears. Due to the continuous slip and climbing of dislocations, the small-angle grain boundaries gradually change to large-angle grain boundaries, the average grain orientation difference increases, the proportion of low coincidence site lattice grain boundaries increases, and the intergranular corrosion resistance of the alloy is enhanced.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17

Similar content being viewed by others

References

  1. R. Chen, Q. Xu, and B. Liu, Modelling Investigation of Precipitation Kinetics and Strengthening for Needle/rod-shaped Precipitates in Al-Mg-Si Alloys, Acta Metall. Sin., 2016, 52(8), p 987–999.

    CAS  Google Scholar 

  2. N. Read, W. Wang, K. Essa, and M.M. Attallah, Selective Laser Melting of AlSi10Mg Alloy: Process Optimisation and mechanical properties development, Mater. Des., 2015, 65, p 417–424.

    Article  CAS  Google Scholar 

  3. L. Zhuo, Z. Wang, H. Zhang, E. Yin, Y. Wang, T. Xu, and C. Li, Effect of Post-process Heat Treatment on Microstructure and Properties of Selective Laser Melted AlSi10Mg Alloy, Mater. Lett., 2019, 234, p 196–200.

    Article  CAS  Google Scholar 

  4. Q. Han and Y. Jiao, Effect of Heat Treatment and Laser Surface Remelting on AlSi10Mg Alloy Fabricated by Selective Laser Melting, Int. J. Adv. Manuf. Technol., 2019, 102(9), p 3315–3324.

    Article  Google Scholar 

  5. Y.J. Liu, H.L. Wang, S.J. Li, S.G. Wang, W.J. Wang, W.T. Hou, and L.C. Zhang, Compressive and Fatigue Behavior of Beta-type Titanium Porous Structures Fabricated by Electron Beam Melting, Acta Mater., 2017, 126, p 58–66.

    Article  ADS  CAS  Google Scholar 

  6. J. Suryawanshi, K.G. Prashanth, and U. Ramamurty, Mechanical Behavior of Selective Laser Melted 316L Stainless Steel, Mater. Sci. Eng. A, 2017, 696, p 113–121.

    Article  CAS  Google Scholar 

  7. R. Baitimerov, P. Lykov, D. Zherebtsov, L. Radionova, A. Shultc, and K.G. Prashanth, Influence of Powder Characteristics on Processability of AlSi12 Alloy Fabricated by Selective Laser Melting, Mater., 2018, 11(5), p 742.

    Article  Google Scholar 

  8. Q. Han, R. Mertens, M.L. Montero-Sistiaga, S. Yang, R. Setchi, K. Vanmeensel, and H. Fan, Laser Powder Bed Fusion of Hastelloy X: Effects of Hot Isostatic Pressing and the Hot Cracking Mechanism, Mater. Sci. Eng. A, 2018, 732, p 228–239.

    Article  CAS  Google Scholar 

  9. P. Wei, Z. Wei, Z. Chen, J. Du, Y. He, J. Li, and Y. Zhou, The AlSi10Mg Samples Produced by Selective Laser Melting: Single Track, Densification, Microstructure and Mechanical Behavior, Appl. Surf. Sci., 2017, 408, p 38–50.

    Article  ADS  CAS  Google Scholar 

  10. L.F. Wang, J. Sun, X.L. Yu, Y. Shi, X.G. Zhu, L.Y. Cheng, and L.J. Guo, Enhancement in Mechanical Properties of Selectively Laser-Melted AlSi10Mg Aluminum Alloys by T6-like Heat Treatment, Mater. Sci. Eng. A, 2018, 734, p 299–310.

    Article  CAS  Google Scholar 

  11. W. Li, S. Li, J. Liu, A. Zhang, Y. Zhou, Q. Wei, and Y. Shi, Effect of Heat Treatment on AlSi10Mg Alloy Fabricated by Selective Laser Melting: Microstructure Evolution, Mechanical Properties and Fracture Mechanism, Mater. Sci. Eng. A, 2016, 663, p 116–125.

    Article  CAS  Google Scholar 

  12. A. Iturrioz, E. Gil, M.M. Petite, F. Garciandia, A.M. Mancisidor, and S.M. San, Selective Laser Melting of AlSi10Mg Alloy: Influence of Heat Treatment Condition on Mechanical Properties and Microstructure, Weld. World, 2018, 62(4), p 885–892.

    Article  CAS  Google Scholar 

  13. S.Z. Uddin, L.E. Murr, C.A. Terrazas, P. Morton, D.A. Roberson, and R.B. Wicker, Processing and Characterization of Crack-free Aluminum 6061 using High-temperature Heating in Laser Powder Bed Fusion Additive Manufacturing, Add Manuf., 2018, 22, p 405–415.

    CAS  Google Scholar 

  14. K.G. Prashanth, S. Scudino, and J. Eckert, Defining the Tensile Properties of Al-12Si Parts Produced by Selective Laser Melting, Acta Mater., 2017, 126, p 25–35.

    Article  ADS  CAS  Google Scholar 

  15. G. Yu, D. Gu, D. Dai, C. Ma, and K. Chang, Influence of Processing Parameters on Laser Penetration Depth and Melting/Re-melting Densification during Selective Laser Melting of Aluminum Alloy, Appl. Phys. A, 2016, 122(10), p 891.

    Article  ADS  Google Scholar 

  16. N.T. Aboulkhair, I. Maskery, C. Tuck, I. Ashcroft, and N.M. Everitt, The Microstructure and Mechanical Properties of Selectively Laser Melted AlSi10Mg: The Effect of a Conventional T6-like Heat Treatment, Mater. Sci. Eng., 2016, 667, p 139–146.

    Article  CAS  Google Scholar 

  17. N.T. Aboulkhair, I. Maskery, I. Ashcroft, C. Tuck, and N.M. Everitt, The role of powder properties on the processability of Aluminium alloys in selective laser melting, Lasers Manuf. Confer., 2015, 1-12.

  18. A. Majeed, Y. Zhang, J. Lv, T. Peng, Z. Atta, and A. Ahmed, Investigation of T4 and T6 Heat Treatment Influences on Relative Density and Porosity of AlSi10Mg Alloy Components Manufactured by SLM, Comput. Ind. Eng., 2020, 139, p 106194.

    Article  Google Scholar 

  19. ISO E N, Corrosion of metals and alloys, Determination of resistance to intergranular corrosion of solution heat-treatable aluminium alloys, Br. Stand. Inst., 2005.

  20. N. Takata, H. Kodaira, K. Sekizawa, A. Suzuki, and M. Kobashi, Change in Microstructure of Selectively Laser Melted AlSi10Mg Alloy with Heat Treatments, Mater. Sci. Eng. A, 2017, 704, p 218–228.

    Article  CAS  Google Scholar 

  21. S. Chen, F.H. Tao, and C.Z. Jia, Study on Microstructure and Properties of 18Ni300 Steel Fabricated by Selective Laser Melting, Found. Technol., 2019, 40(07), p 657–661.

    CAS  Google Scholar 

  22. M. Calcagnotto, D. Ponge, E. Demir, and D. Raabe, Orientation Gradients and Geometrically Necessary Dislocations in Ultrafine Grained Dual-phase Steels Studied by 2D and 3D EBSD, Mater. Sci. Eng. A, 2010, 527(10), p 2738–2746.

    Article  Google Scholar 

  23. S.L. Liu, Z.H. **ong, S.F. Li, Y. Shi, Y. Yang, and R.D.K. Misra, Role of Melt Pool Boundary Condition in Determining the Mechanical Properties of Selective Laser Melting AlSi10Mg Alloy, Mater. Sci. Eng. A, 2019, 740, p 148–156.

    Google Scholar 

  24. X. Liu, C. Zhao, X. Zhou, Z. Shen, and W. Liu, Microstructure of Selective Laser Melted AlSi10Mg Alloy, Mater. Des., 2019, 168, p 107677.

    Article  CAS  Google Scholar 

  25. W.C. Li, Y.Z. Zou, and J.M. Zeng, Influence of Solution Temperature and Time on Microstructure of ZL114A Alloy, Mater. Mech. Eng., 2008, 11, p 25–27.

    Google Scholar 

  26. Z.Q.Cµi and Y.C Qin, metallography and heat treatment, China Mac. Press, 2007.

  27. X. Zheng, Effects of different loading paths on microstrµctµre and textµre evolµtion of 7A04 alµminµm alloy, North µniversity of China, 2020.

  28. N. Takata, H. Kodaira, K. Sekizawa, A. Suzuki, and M. Kobashi, Change in Microstrµctµre of Selectively Laser Melted AlSi10Mg Alloy with Heat Treatments, Mater. Sci. Eng. A, 2017, 704, p 218–228.

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This work was financially supported by the Natural Science Foundation of Hunan Province (2023JJ50174), and the Project of Industry-University Cooperation and Collaborative Education of Chinese Ministry of Education (BINTECH-KJZX-20220831-37).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to **aomei Yang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Jian, H., Yang, M., Fang, W. et al. Effect of Heat Treatment on Microstructure and Properties of Selective Laser Melting AlSi10Mg Alloy. J. of Materi Eng and Perform (2024). https://doi.org/10.1007/s11665-024-09271-3

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1007/s11665-024-09271-3

Keywords

Navigation