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Low temperature degradation of alumina-toughened zirconia in artificial saliva

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Abstract

The long-term aging behavior of an alumina-toughened zirconia (ATZ) ceramic in artificial saliva hydrothermal atmosphere was determined and compared with that of tetragonal zirconia polycrystals doped with 3mol% Y2O3 (3Y-TZP). The specimens of 3Y-TZP and ATZ were aged in distilled water and artificial salivary respectively at 134 °C. Monoclinic phase content was evaluated by X-ray diffraction (XRD) analysis. Specimen strength was determined by a biaxial bending test. Surface screening was done using an atomic force microscope (AFM). No statistically significant influence of any treatment on strength was demonstrated for either material. However, XRD measurements revealed ATZ’s anti-aging properties were much better than TZP after the aging treatment. Therefore, ATZ can be applied to the field of dentistry. Artificial saliva in ceramic surface sediments may be useful for strengthening ceramics.

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References

  1. Chevalier J. What Future for Zirconia as a Biomaterial[J]? Biomaterials, 2006, 27(4): 535–543

    Article  CAS  Google Scholar 

  2. Garvie RC, HR, Pascoe RT. Ceramic Steel[J]. Nature, 1975, 258: 703

    Article  CAS  Google Scholar 

  3. Lawson S. Environmental Degradation of Zirconia Ceramics[J]. Journal of the European Ceramic Society, 1995, 15(6): 485–502

    Article  CAS  Google Scholar 

  4. Cattani-Lorente M, Scherrer SS, Ammann P, et al. Low Temperature Degradation of a Y-TZP Dental Ceramic[J]. Acta Biomaterialia, 2011, 7(2): 858–865

    Article  CAS  Google Scholar 

  5. Sato T and Shimada M. Transformation of Yttria-Doped Tetragonal ZrO2 Polycrystals by Annealing in Water[J]. Journal of the American Ceramic Society, 1985, 68(6): 356–356

    Article  CAS  Google Scholar 

  6. Swab JJ. Low Temperature Degradation of Y-TZP Materials[J]. Journal of Materials Science, 1991, 26(24): 6 706–6 714

    Article  CAS  Google Scholar 

  7. Payyapilly JJ and DP Butt. Kinetics of Hydrothermally Induced Transformation of Yttria Partially Stabilized Zirconia[J]. Journal of Nuclear Materials, 2007, 360(2): 92–98

    Article  CAS  Google Scholar 

  8. Chevalier J, AHD Aza, Fantozzi G, et al. Extending the Lifetime of Ceramic Orthopaedic Implants[J]. Advanced Materials, 2000, 12(21): 1 619–1 621

    Article  CAS  Google Scholar 

  9. Schneider J, Begand S, Kriegel R, et al. Low-Temperature Aging Behavior of Alumina-Toughened Zirconia[J]. Journal of the American Ceramic Society, 2008, 91(11): 3 613–3 618

    Article  CAS  Google Scholar 

  10. Gutknecht D, Chevalier J, Garnier V, et al. Key Role of Processing to Avoid Low Temperature Ageing in Alumina Zirconia Composites for Orthopaedic Application[J]. Journal of the European Ceramic Society, 2007. 27(2–3): 1 547–1 552

    CAS  Google Scholar 

  11. Herrmann M, Seipel B, Schilm J, et al. Hydrothermal Corrosion of Zirconia-toughened Alumina (ZTA) at 200 Degrees C[J]. Journal of the European Ceramic Society, 2005, 25(10): 1 805–1 812

    Article  CAS  Google Scholar 

  12. Tsubakino H, Sonoda K and Nozato R. Martensite Transformation Behaviour During Isothermal Ageing in Partially Stabilized Zirconia with and Without Alumina Addition[J]. Journal of Materials Science Letters, 1993, 12(3): 196–198

    Article  CAS  Google Scholar 

  13. Marino CEB and Mascaro LH. EIS Characterization of a Ti-dental Implant in Artificial Saliva Media: Dissolution Process of the Oxide Barrier[J]. Journal of Electroanalytical Chemistry, 2004, 568(1–2): 115–120

    Article  CAS  Google Scholar 

  14. ISO/TR 11405. Guidance on Testing of Adhesion to Tooth Structure in Dental Materials[S]. 1994

    Google Scholar 

  15. Chevalier J, Cales B and Drouin JM. Low-Temperature Aging of Y-TZP Ceramics[J]. Journal of the American Ceramic Society, 1999, 82(8): 2 150–2 154

    CAS  Google Scholar 

  16. Lughi V and Sergo V. Low Temperature Degradation-aging-of zirconia: A Critical Review of the Relevant Aspects in Dentistry[J]. Dental Materials, 2010, 26(8): 807–820

    Article  CAS  Google Scholar 

  17. Yoshimura M, Noma T, Kawabata K, et al. Role of H2O on the Degradation Process of Y-TZP[J]. Journal of Materials Science Letters, 1987, 6(4): 465–467

    Article  CAS  Google Scholar 

  18. Chevalier J, Gremillard L, Virkar AV, et al. The Tetragonal-Monoclinic Transformation in Zirconia: Lessons Learned and Future Trends[J]. Journal of the American Ceramic Society, 2009, 92(9): 1901–1920

    Article  CAS  Google Scholar 

  19. Pezzotti G, Saito T, Padeletti G, et al. Nano-scale Topography of Bearing Surface in Advanced Alumina/zirconia Hip Joint Before and After Severe Exposure in Water Vapor Environment[J]. Journal of Orthopaedic Research, 2010, 28(6): 762–766

    CAS  Google Scholar 

  20. Papanagiotou HP, Morgano SM, Giordano RA, et al. In vitro Evaluation of Low-temperature Aging Effects and Finishing Procedures on the Flexural Strength and Structural Stability of Y-TZP Dental Ceramics[J]. The Journal of Prosthetic Dentistry, 2006, 96(3): 154–164

    Article  CAS  Google Scholar 

  21. Borchers L, Stiesch M, Bach F-W, et al. Influence of Hydrothermal and Mechanical Conditions on the Strength of Zirconia[J]. Acta Biomaterialia, 2010, 6(12): 4 547–4 552

    Article  CAS  Google Scholar 

  22. Ardlin BI. Transformation-toughened Zirconia for Dental Inlays, Crowns and Bridges: Chemical Stability and Effect of Low-temperature Aging on Flexural Strength and Surface Structure[J]. Dental Materials, 2002, 18(8): 590–595

    Article  CAS  Google Scholar 

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Correspondence to Wei Li  (**伟).

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Funded by the National High-Tech Research and Development Program of China (863 Program) (No. 2006AA03Z440)

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Zhao, Y., Jiang, L., Liao, Y. et al. Low temperature degradation of alumina-toughened zirconia in artificial saliva. J. Wuhan Univ. Technol.-Mat. Sci. Edit. 28, 844–848 (2013). https://doi.org/10.1007/s11595-013-0780-8

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  • DOI: https://doi.org/10.1007/s11595-013-0780-8

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