SpringerLink
Log in

Electron beam-induced formation of nanosized α-Fe crystals

  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Focused electron beam induced chemical vapor deposition was performed in a scanning electron microscope with a field emission gun using a precursor of iron carbonyl. Due to the longer deposition time and higher gas pressure than those of our previous electron beam-induced deposition method, a new type of deposition occurred. A large amount of nanosized crystals were produced around the focused beam irradiation point on a carbon substrate at room temperature. The nanocrystals were systematically characterized using transmission electron microscopy with electron energy loss spectroscopy (EELS), and were identified to be single crystals of α-Fe.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price includes VAT (Germany)

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. S. W. Jung, W. I. Park, G. C. Yi and M. Kim, Adv. Mat. 15 (2003) 1358.

    Article  CAS  Google Scholar 

  2. D. G. Shchukin, I. L. Radtchenko and G. B. Sukhorukov, J. Phys. Chem. B 107 (2003) 86.

    Article  CAS  Google Scholar 

  3. M. Shimojo, M. Takeguchi, M. Tanaka, K. Mitsuishi and K. Furuya, Appl. Phys. A 79 (2004) 1869.

    Article  CAS  Google Scholar 

  4. M. Tanaka, M. Shimojo, K. Mitsuishi and K. Furuya, ibid. 78 (2004) 543.

    CAS  Google Scholar 

  5. K. Mitsuishi, M. Shimojo, M. Han and K. Furuya, Appl. Phys. Lett. 83 (2003) 2064.

    Article  CAS  Google Scholar 

  6. N. Silvis-Cividjian, C. W. Hagen, P. Kruit, M. A. J. van der Stam and H. B. Groen, ibid. 82 (2003) 3514.

    CAS  Google Scholar 

  7. I. Utke, A. Luisier, P. Hoffmann, D. Laub and P. A. Buffat, ibid. 81 (2002) 3245.

    CAS  Google Scholar 

  8. K. Ueda and M. Yoshimura, Thin Solid Films 464/465 (2004) 331.

    Article  Google Scholar 

  9. P. C. Engelking and W. C. Lineberger, J. Am. Chem. Soc. 101 (1979) 5569.

    Article  CAS  Google Scholar 

  10. K. E. Lewis, D. M. Golden and G. P. Smith, ibid. 106 (1984) 3905.

    CAS  Google Scholar 

  11. J. Phillips and J. A. Dumesic, Appl. Surf. Sci. 7 (1981) 215.

    Article  CAS  Google Scholar 

  12. J. S. Foord and R. B. Jackman, Chem. Phys. Lett. 112 (1984) 190.

    Article  CAS  Google Scholar 

  13. J. R. Swanson, C. M. Friend and Y. J. Chabal, J. Vac. Sci. Technol. A 6 (1988) 770.

    Article  Google Scholar 

  14. H. W. P. Koops, A. Kaya and M. Weber, J. Vac. Sci. Technol. B 13 (1995) 2400.

    Article  CAS  Google Scholar 

  15. R. R. Kunz and T. M. Mayer, ibid. 6 (1988) 1557.

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. High Voltage Electron Microscopy Station, National Institute for Materials Science, 3-13 Sakura, Tsukuba, 305-0003, Japan

    W. Zhang, M. Shimojo, M. Takeguchi & K. Furuya

  2. Precision and Intelligence Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori, Yokohama, 226-8503, Japan

    M. Shimojo

Authors
  1. W. Zhang
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. Shimojo
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. Takeguchi
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. K. Furuya
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to W. Zhang.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Zhang, W., Shimojo, M., Takeguchi, M. et al. Electron beam-induced formation of nanosized α-Fe crystals. J Mater Sci 41, 2577–2580 (2006). https://doi.org/10.1007/s10853-006-7783-1

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10853-006-7783-1

Keywords

Search

Navigation