SpringerLink
Log in

Preparation and characterization of surface energy of BPDA-BAPP polyimide

  • Published:
Macromolecular Research Aims and scope Submit manuscript

Abstract

The surface properties (water sorption and repellency, adhesion) are closely related to the surface tension of polymer solids. The critical surface tension (γ c ) and surface tension (γ s ) of a polymer solid were estimated by the contact angle method by our quantitative imaging system. BPDA (3,3′,4,4′-biphenyl tetracarboxylic dianhydride)-BAPP (1,3-Bis(4-aminophenoxy) propane) polyimide was successfully synthesized. Theγ c values were analyzed by a Zisman plot, a Young-Dupré-Good-Girifalco plot, and a log (1+cos θ) vs logγ L plot. Theγ s value of BPDA-BAPE polyimide was evaluated using the geometric mean equation and our multiple regression analysis. The calculated values ofγ d S (a dispersion component),γ p S (a polar component),γ h S (a hydrogen bonding component), andγ S were 30.79, 9.32, 0.20, and 40.31 mN·m-1, respectively. Theγ S of BPDA-BAPP polyimide containing both a methylene group and an ether group was larger than that of the polyimide containing only a methylene group.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price includes VAT (Germany)

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. W. S. Ruska,Microelectronic Processing: An Introduction to the Manufacture of Integrated Circuits, McGraw-Hill, New York, 1987, pp 68–76.

    Google Scholar 

  2. A. Endo, M. Takada, K. Adachi, H. Takasago, T. Yada, and Y. Onishl,J. Electrochem. Soc.: Solid-State Sci. Tech.,34, 2522 (1987).

    Google Scholar 

  3. K. L. Mittal,Polyimides: synthesis, characterization, and applications, Plenum Press, New York, 1984.

    Google Scholar 

  4. C. Feger, M. M. Khojasteh, and M. S. Htoo,Advances in polyimide science and technology, Technomic Publications, Lancaster, 1993.

    Google Scholar 

  5. C. E. Sroog,J. Polym. Sci.: Macromol. Rev.,11, 161 (1979).

    Article  Google Scholar 

  6. A. M. Wilson,Use of Polyimides in VLSI fabrication, in Polyimides, 1st ed., K. L. Mittal, Ed., Plenum Press, New York, 1984, pp 715–733.

    Google Scholar 

  7. A. M. Wilson,Thin Solid Films,83, 145 (1981).

    Article  CAS  Google Scholar 

  8. E. Sacher and J. R. Susko,J. Appl. Polym. Sci.,26, 679 (1981).

    Article  CAS  Google Scholar 

  9. M. Ree, M. J. Goldberg, G. Czornyj, H. S. Han, and C. C. Gryte,Polym. Mater. Sci. Eng.,68, 126 (1993).

    CAS  Google Scholar 

  10. D. H. Lee,Polymer(Korea),11, 206 (1987).

    CAS  Google Scholar 

  11. F. Belluchi, I. Khamis, S. D. Senturia, and R. M. Lantanison,J. Electrochem. Soc.,137, 1778 (1990).

    Article  Google Scholar 

  12. B. S. Kim, S. H. Bae, Y. H. Park, and J.-H. Kim,Macromol. Res.,15, 357 (2007).

    CAS  Google Scholar 

  13. A. S. Mathew, I. Kim, and C. S. Ha,Macromol. Res.,15, 114 (2007).

    Article  Google Scholar 

  14. H. S. Lee, A. Roy, A. S. Badami, and J. E. McGrath,Macromol. Res.,15, 160 (2007).

    Article  CAS  Google Scholar 

  15. H. S. Han, Ph. D. Thesis, Columbia University, New York, 1993.

    Google Scholar 

  16. D. D. Denton, D. R. Day, D. F. Priore, and S. D. Senturia,J. Electron. Mater.,14, 119 (1985).

    Article  CAS  Google Scholar 

  17. J. Melcher, Y. Deben, and G. Arlt,IEEE Elecrt. Insul.,24, 31 (1989).

    Article  CAS  Google Scholar 

  18. E. Sacherand and J. R. Sucko,J. Appl. Polym. Sci.,23, 2355 (1979).

    Article  Google Scholar 

  19. H. J. Merrem, R. Klug, and H. Hartner,New Developments in Photosensitive Polyimide, in Polyimides, 2nd ed., K. L. Mittal, Ed., Plenum Press, New York, 1989, pp 919–931.

    Google Scholar 

  20. E. Tchangai, Y. Segui, and K. Doukkali,J. Appl. Polym. Sci.,38, 305 (1989).

    Article  CAS  Google Scholar 

  21. J.-H. Jou, R. Huang, P.-T. Huang, and W.-P. Shen,J. Appl. Polym. Sci.,43, 857 (1991).

    Article  CAS  Google Scholar 

  22. Y. Kwon and K.-H. Kim,Macromol. Res.,14, 424 (2006).

    Article  CAS  Google Scholar 

  23. M. Ree,Macromol. Res.,14, 1 (2006).

    Article  CAS  Google Scholar 

  24. S. J. Shin, J. H. Chi, W. C. Zin, T. Chang, M. Ree, and J. C. Jung,Polymer(Korea),30, 97 (2006).

    CAS  Google Scholar 

  25. M. Ree, T. J. Shin, and S. W. Lee,Korea Polym. J.,9, 1 (2001).

    CAS  Google Scholar 

  26. M. Ree, T. J. Shin, Y. H. Park, H. Lee, and T. Chang,Korea Polym. J.,7, 370 (1999).

    CAS  Google Scholar 

  27. W. H. Goh, K. Kim, and M. Ree,Korea Polym. J.,6, 241 (1998).

    CAS  Google Scholar 

  28. H. Han and M. Ree,Korea Polym. J.,5, 152 (1997).

    CAS  Google Scholar 

  29. H. W. Fox and W. A. Zisman,J. Colloid Sci.,5, 514 (1950).

    Article  CAS  Google Scholar 

  30. R. E. Johnson and R. H. Dettre,J. Colloid Sci.,20, 73 (1965).

    Google Scholar 

  31. A. M. Gaudin,Flotation, McGraw-Hill, New York, 1957, p. 163.

    Google Scholar 

  32. A. W. Adams, F. P. Shirley, and K. T. Kunichika,J. Colloid Interf. Sci.,34, 461 (1970).

    Article  Google Scholar 

  33. T. Fort and H. T. Patterson,J. Colloid Sci.,18, 217 (1963).

    Article  CAS  Google Scholar 

  34. Y. Kitazaki and T. J. Hata,J. Adhes. Soc. Jpn.,8, 131 (1972).

    CAS  Google Scholar 

  35. Y. Kano and S. Akiyama,Polymer,33, 1690 (1992).

    Article  CAS  Google Scholar 

  36. H. W. Fox and W. A. Zisman,J. Colloid Sci.,7, 109 (1952a).

    Article  CAS  Google Scholar 

  37. H. W. Fox and W. A. Zisman,J. Colloid Sci.,7, 428 (1952b).

    Article  CAS  Google Scholar 

  38. A. Zisman, inTreaties on Contact Angle, Wettability and Adhesion, Advances in Chemistry Series, American Chemical Society, Washington DC, 1964, No. 43, pp 1–51.

    Book  Google Scholar 

  39. F. M. Fowkes, inTreaties on Contact Angle, Wettability and Adhesion, Advances in Chemistry Series, American Chemical Society, Washington DC, 1964, No. 43, pp 99–111.

    Google Scholar 

  40. R. J. Good, inTreaties on Contact Angle, Wettability and Adhesion, Advances in Chemistry Series, American Chemical Society, Washington DC, 1964, No. 43, pp 74–87.

    Book  Google Scholar 

  41. R. J. Good, inTreaties on Adhesion and Adhesive, R. L. Patrick, Ed., Marcel Dekker, New York, 1967, Vol. 1, pp 9–68.

    Google Scholar 

  42. R. J. Good and L. A. Girifalco,J. Phys. Chem.,64, 561 (1960).

    Article  CAS  Google Scholar 

  43. Y. Kano and T. Saito,Setchaku,32, 396 (1988).

    CAS  Google Scholar 

  44. S. Wu,Polymer Interface and Adhesion, Marcel Dekker, New York, 1982a, p 105.

    Google Scholar 

  45. D. H. Kaelble and K. C. Uy,J. Adhes.,2, 51 (1970).

    Google Scholar 

  46. S. Wu,Polymer Interface and Adhesion, Marcel Dekker, New York, 1982b, pp 257–259.

    Google Scholar 

  47. A. W. Adamson,Physical Chemistry of Surfaces, 5th ed., John Wiley & Sons, New York, 1990a, pp 389–392.

    Google Scholar 

  48. M. K. Ghosh and K. L. Mittal,Polyimides: Fundamentals and Applications, Marcel Dekker, New York, 1996, pp 16–18.

    Google Scholar 

  49. S. Wu,Polymer Interface and Adhesion, Marcel Dekker, New York, 1982c, p. 162.

    Google Scholar 

  50. S. Wu,Polymer Interface and Adhesion, Marcel Dekker, New York, 1982d, p. 183.

    Google Scholar 

  51. A. W. Adamson,Physical Chemistry of Surfaces, 5th ed., John Wiley & Sons, New York, 1990b, pp 397–398.

    Google Scholar 

  52. W. Gutowski,J. Adhes.,19, 29 (1985).

    Article  Google Scholar 

  53. K.-H. Kim and Y. Kwon,J. Chem. Eng. Jpn.,38, 641 (2005)

    Article  CAS  Google Scholar 

  54. K.-H. Kim, Y.-G. Kim, and Y. Kwon,Mol. Cryst. Liq. Cryst.,470, 145 (2007).

    Article  CAS  Google Scholar 

  55. J. Brandrup and E. H. Immergut,Polymer Handbook, 3rd ed., Wiley-Interscience, John Wiley & Sons, New York, 1989, p VI/422.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Chemical Engineering, Daegu University, 712-714, Gyungbuk, Korea

    Kyung-Hoe Kim, Yong-Gwon Kim & Younghwan Kwon

Authors
  1. Kyung-Hoe Kim
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Yong-Gwon Kim
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Younghwan Kwon
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Kyung-Hoe Kim.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kim, KH., Kim, YG. & Kwon, Y. Preparation and characterization of surface energy of BPDA-BAPP polyimide. Macromol. Res. 17, 388–396 (2009). https://doi.org/10.1007/BF03218879

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF03218879

Keywords

Search

Navigation