Abstract
The thermally initiated cyclocondensation of 1,3-dimethyl-4-alkylamino-5-nitrosouracils (I), giving rise to the 8-substituted theophyllines (II), was studied by DSC. The corresponding reaction enthalpies were determined for six derivatives of I.
References
M. M. Barbooti, D. A. Al-Sammerrai and R. M. Al-Ansari, Thermochim. Acta, 79 (1984) 139.
H. Masuda, T. Kawarada, K. Myiokawa and I. Masuda, Thermochim. Acta, 63 (1983) 307.
D. J. Whelan, R. J. Spear and R. W. Read, Thermochim. Acta, 80 (1984) 149.
J. M. Barton, Thermochim. Acta, 71 (1983) 337.
C. W. Bird, I. J. Partridge and C. K. Wong, Tetrahedron, 37 (1981) 1011.
J. M. Salas-Peregrin, E. Colacio-Rodriguez, M. A. Romero-Molina and M. P. Sanchez-Sanchez, Thermochim. Acta, 69 (1983) 313.
M. N. Moreno-Carretero and J. M. Salas-Peregrin, J. Thermal Anal., 29 (1984) 1053.
H. Goldner, G. Dietz and E. Carstens, Belg. Patent 616174 (1962), VEB Arzneimittelwerk Dresden.
P. Králik, L. Štibrányi, T. Gondová and M. Hirjak, Proc. 8th ICTA Bratislava, Vol. 2, 1985, p. 44.
T. Gondová and P. Králik, in preparation.
W. E. Brown, D. Dollimore and A. K. Galwey, Comprehensive Chemical Kinetics, Vol. 22, Elsevier, Amsterdam.
A. W. Coats and J. P. Redfern, Nature (London), 201 (1964) 68.
Author information
Authors and Affiliations
Additional information
The authors are grateful to Professor R. Domansky for a careful reading of the manuscript and for helpful suggestions.
Rights and permissions
About this article
Cite this article
Králik, P., Gondová, T. & Štibrányi, L. Thermal behaviour of 1,3-dimethyl-4-alkylamino-5-nitrosouracils. Journal of Thermal Analysis 31, 173–175 (1986). https://doi.org/10.1007/BF01913898
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF01913898